Here is the original GKN patent:
http://worldwide.espacenet.com/publicationDetails/originalDocument?CC=US&NR=4022084A&KC=A&FT=D&date=19770510&DB=EPODOC&locale=nl_NLIt makes interesting reading.
The GKN people knew that it worked, but did not know why ....
The original silicone oil also came from Dow Corning ....
Some statements about filling in it too.
The coupler starts really doing something once 100% fill rate is reached due to thermal expansion. So fill it 100% and don't close it. Warm it up to 212F and the excess goop will flow out. Then close the coupler. Now you know that you have a coupler that starts working from 212F. Easy peasy.
Roy Lunn must have done the same experiments and came to a 70% fill rate.
I would do it like this:
Clean the internals with white spirit.
Then fill it to the brim with white spirit.
Empty it in a glass measuring cup (from the kitchen) and make a note of the level.
Use the same cup and fill it with silicone oil 70% of the previous measurement and put that in the viscous coupler.
Why not use the silicone oil to do the measurement? It is too goopy, it won't come out again.
So better use something nice and thin like white spirit.